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Jamalipour, Parisa, Choobkar, Nasrin, Abrishamkar, Maryam, Pournamdari, Elham. (1401). Designed a Fluorescent Method by Using PbS with Gelatin via Quantum Dots for the Determination of Amount Insecticide toxic Fenpyroximate in Water Samples. فصلنامه علمی زیست فناوری گیاهان زراعی, 9(2), 28-37. doi: 10.30473/ijac.2022.64566.1239
Parisa Jamalipour; Nasrin Choobkar; Maryam Abrishamkar; Elham Pournamdari. "Designed a Fluorescent Method by Using PbS with Gelatin via Quantum Dots for the Determination of Amount Insecticide toxic Fenpyroximate in Water Samples". فصلنامه علمی زیست فناوری گیاهان زراعی, 9, 2, 1401, 28-37. doi: 10.30473/ijac.2022.64566.1239
Jamalipour, Parisa, Choobkar, Nasrin, Abrishamkar, Maryam, Pournamdari, Elham. (1401). 'Designed a Fluorescent Method by Using PbS with Gelatin via Quantum Dots for the Determination of Amount Insecticide toxic Fenpyroximate in Water Samples', فصلنامه علمی زیست فناوری گیاهان زراعی, 9(2), pp. 28-37. doi: 10.30473/ijac.2022.64566.1239
Jamalipour, Parisa, Choobkar, Nasrin, Abrishamkar, Maryam, Pournamdari, Elham. Designed a Fluorescent Method by Using PbS with Gelatin via Quantum Dots for the Determination of Amount Insecticide toxic Fenpyroximate in Water Samples. فصلنامه علمی زیست فناوری گیاهان زراعی, 1401; 9(2): 28-37. doi: 10.30473/ijac.2022.64566.1239

Designed a Fluorescent Method by Using PbS with Gelatin via Quantum Dots for the Determination of Amount Insecticide toxic Fenpyroximate in Water Samples

Iranian Journal of Analytical Chemistry
دوره 9، شماره 2 - شماره پیاپی 18، آذر 2022، صفحه 28-37    اصل مقاله (1.23 M)
نوع مقاله: Full research article
شناسه دیجیتال (DOI): 10.30473/ijac.2022.64566.1239
نویسندگان
Parisa Jamalipour1؛ Nasrin Choobkar1؛ Maryam Abrishamkar* 2؛ Elham Pournamdari3
1Department of Environment, Kermanshah Branch, Islamic Azad University, Kermanshah, Iran
2Department of Chemistry, Ahvaz Branch, Islamic Azad University, Ahvaz, Iran
3Department of Chemistry, Islamshahr Branch, Islamic Azad University, Islamshahr, Iran
چکیده
In this current article, a chemical sensor was synthesized PbS functionalized with Gelatin Quantum Dots for Fenpyroximate. The measure of Fenpyroximate was performed using concentration (2.5×10-3 mol L-1), PbS Quantum Dot-Gelatin nanocomposites sensor, pH 6, and time 40 s, wavelength 328 nm. Under the optimum conditions, the detection limit linear range were obtained (0.02 to 20.0 µg L-1). The standard deviation of less than (2.0%), and detection limits (3S/m) of the method (0.02 µg L-1) for determination of Fenpyroximate, was obtained. The observed outcomes confirmed the suitability recovery and a very low detection limit for measuring the Fenpyroximate. The chemical PbS Quantum Dot–Gelatin nanocomposites sensor as excellent sensor in the practical application of Fenpyroximate related to residue management is in surface water samples.
کلیدواژه‌ها
Fenpyroximate؛ Insecticide؛ Fluorescence؛ Sensor؛ Quantum Dots
عنوان مقاله [English]
طراحی یک روش فلورسنت با استفاده از سولفید سرب با ژلاتین از طریق نقاط کوانتومی برای تعیین مقدار حشره‌کش فنی ‌پیروکسی میت در نمونه‌های آب
نویسندگان [English]
پریسا جمالی پور1؛ نسرین چوبکار1؛ مریم ابریشمکار2؛ الهام پورنامداری3
1گروه مهندسی کشاورزی گرایش محیط زیست، دانشگاه آزاد اسلامی، واحد کرمانشاه، کرمانشاه، ایران
2گروه شیمی، دانشگاه آزاد اسلامی، واحد اهواز، اهواز، ایران
3گروه شیمی، دانشگاه آزاد اسلامی، واحد اسلامشهر، اسلامشهر، ایران
چکیده [English]
در این مقاله، یک حسگر شیمیایی سولفید سرب سنتز شد که با نقاط کوانتومی ژلاتین برای فنی ‌پیروکسی میت عامل‌دار شده است. اندازه گیری فنی ‌پیروکسی میت با استفاده از غلظت (3-10×5/2 مولار)، سنسور نانوکامپوزیت نقطه کوانتومی سولفید سرب-ژلاتین، 6=pH  و زمان 40 ثانیه، طول موج 328 نانومتر انجام شد. در شرایط بهینه، محدوده خطی حد تشخیص (02/0 تا 0/20 میکروگرم در لیتر) به دست آمد. انحراف استاندارد (LOD) کمتر از (0/2 درصد)، و محدودیت های تشخیص روش (02/0 میکروگرم در لیتر) برای تعیین فنی ‌پیروکسی میت، بدست آمد. نتایج مشاهده‌شده بازیابی مناسب و حد تشخیص بسیار پایین برای اندازه‌گیری فنی ‌پیروکسی میت را تأیید کرد. حسگر نانوکامپوزیت نقطه کوانتومی سولفید سرب-ژلاتین به عنوان حسگر عالی در کاربرد عملی فنی ‌پیروکسی میت مربوط به مدیریت پسماند در نمونه‌های آب سطحی است.
کلیدواژه‌ها [English]
فنی پیروکسی میت, حشره‌کش, فلوئورسانس, حسگر, اتصالات کوانتومی عرضی
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آمار
تعداد مشاهده مقاله: 333
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