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Dehno Khalaji, Aliakbar, Gharib, Fatemeh. (1395). Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride. فصلنامه علمی زیست فناوری گیاهان زراعی, 4(Issue 3, pp. 236-358, Serial No. 12), 265-272.
Aliakbar Dehno Khalaji; Fatemeh Gharib. "Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride". فصلنامه علمی زیست فناوری گیاهان زراعی, 4, Issue 3, pp. 236-358, Serial No. 12, 1395, 265-272.
Dehno Khalaji, Aliakbar, Gharib, Fatemeh. (1395). 'Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride', فصلنامه علمی زیست فناوری گیاهان زراعی, 4(Issue 3, pp. 236-358, Serial No. 12), pp. 265-272.
Dehno Khalaji, Aliakbar, Gharib, Fatemeh. Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride. فصلنامه علمی زیست فناوری گیاهان زراعی, 1395; 4(Issue 3, pp. 236-358, Serial No. 12): 265-272.

Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride

Iranian chemical communication
مقاله 16، دوره 4، Issue 3, pp. 236-358, Serial No. 12، مهر 2016، صفحه 265-272    اصل مقاله (278.15 K)
نوع مقاله: Original Research Article
نویسندگان
Aliakbar Dehno Khalaji* ؛ Fatemeh Gharib
Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran
چکیده
In this paper, nickel oxide (NiO) nanoparticles have been prepared by solid state thermal decomposition of an acyclic nickel(II) complex (1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II) chloride, [NiL]Cl2, in an electrical furnace at optimal temperature, 450 ºC for 3.5 h. The nickel(II) complex is obtained via solid state synthesis using nickel(II) chloride and tetradentate O4 acyclic ligand 1,2-bis(2-formyl-3-methoxyphenyl)propane. The structure and morphology of NiO nanoparticles are characterized by Fourier transform infrared spectroscopy (FT-IR), powder X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). XRD and TEM analysis show that NiO nanoparticles have pure and cubic phase with the average size of 5-10 nm.
کلیدواژه‌ها
Nickel oxide؛ nanoparticles؛ Solid state؛ nickel(II) complex
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