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Banaei, Alireza, Karimi, Soheyla, Nurbageri, Negar. (1395). Synthesis and characterization of 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-one. فصلنامه علمی زیست فناوری گیاهان زراعی, 4(Issue 4, pp. 359-490, Serial No. 13), 359-363.
Alireza Banaei; Soheyla Karimi; Negar Nurbageri. "Synthesis and characterization of 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-one". فصلنامه علمی زیست فناوری گیاهان زراعی, 4, Issue 4, pp. 359-490, Serial No. 13, 1395, 359-363.
Banaei, Alireza, Karimi, Soheyla, Nurbageri, Negar. (1395). 'Synthesis and characterization of 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-one', فصلنامه علمی زیست فناوری گیاهان زراعی, 4(Issue 4, pp. 359-490, Serial No. 13), pp. 359-363.
Banaei, Alireza, Karimi, Soheyla, Nurbageri, Negar. Synthesis and characterization of 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-one. فصلنامه علمی زیست فناوری گیاهان زراعی, 1395; 4(Issue 4, pp. 359-490, Serial No. 13): 359-363.

Synthesis and characterization of 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-one

Iranian chemical communication
مقاله 22، دوره 4، Issue 4, pp. 359-490, Serial No. 13، دی 2016، صفحه 359-363    اصل مقاله (206.72 K)
نوع مقاله: Short communication
نویسندگان
Alireza Banaei* ؛ Soheyla Karimi؛ Negar Nurbageri
Department of Chemistry, Payame Noor University, PB BOX 19395-4697 Tehran, Iran
چکیده
New 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-one (2a) was synthesized in good yield by the Petrenko–Kritchenko reaction of 2, 2'-((3-hydroxypropane-1, 2-diyl) bis (oxy)) bisbenzaldehyde (1a) with diethyl ketone in the mixture of ethanol and acetic acid as solvent in the presence of ammonium acetate. The compounds were characterized by elemental analyses, IR, 1H-NMR, 13C-NMR and mass spectrometry.
Keywords: Petrenko–Kritchenko condensation, Macrocyclic compound, Bisaldehyde, 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-one, 2, 2'-((3 hydroxypropane-1, 2-diyl) bis (oxy)) bisbenzaldehyde
کلیدواژه‌ها
Petrenko-Kritchenko condensation؛ macrocyclic compound؛ bisaldehyde
مراجع
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