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Silica bonded n-propyl-1,3,5-triazine-2,4,6-triamine as a basic catalyst for synthesis of arylmethylenemalononitrile and pyran annulated heterocyclic compounds | ||
Iranian chemical communication | ||
مقاله 11، دوره 5، Issue 4, pp. 364-493, Serial No. 17، دی 2017، صفحه 471-483 اصل مقاله (793.31 K) | ||
نوع مقاله: Original Research Article | ||
نویسندگان | ||
Jamal Davarpanah* 1؛ Afzal Zafarpour2؛ Behrooz Tayebi2 | ||
1Production Technology Research Institute (ACECR), Ahwaz, Iran. | ||
2Chemistry Department, Omidiyeh Branch of Islamic Azad University, Omidiyeh, Iran | ||
چکیده | ||
In the present research, silica bonded n-propyl-1,3,5-triazine-2,4,6-triamine (SPTT) was synthesized by direct incorporation of chloropropyl groups through co-condensation of tetraethyl orthosilicate (TEOS) and 3-chloropropyl trimethoxysilane (CPTMS) and subsequent grafting the melamine onto the propyl groups via simple nucleophilic substitution reaction. The catalyst has been characterized by fourier transform infrared spectroscopy (FT-IR) and thermogravimetric analysis (TGA). The catalytic activity of catalyst was probed through synthesis of arylmethylenemalononitrile and pyran annulated heterocyclic compounds.The catalytic activity of catalyst was probed through synthesis of arylmethylenemalononitrile and pyran annulated heterocyclic compounds.The catalytic activity of catalyst was probed through synthesis of arylmethylenemalononitrile and pyran annulated heterocyclic compounds. | ||
کلیدواژهها | ||
Melamine؛ arylmethylenemalononitrile compounds؛ pyran heterocyclic compounds؛ functionalized silica catalyst | ||
مراجع | ||
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