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Vahdat, Seyed Mohammad, Mohammadzadeh, Abbas, Derafshian, Esmaiel, Akhoondi, Somaieh. (1393). Efficient classical synthesis of aminoazines under microwave irradiation. فصلنامه علمی زیست فناوری گیاهان زراعی, 2(Issue 2, pp. 82-163, Serial No. 3), 157-163.
Seyed Mohammad Vahdat; Abbas Mohammadzadeh; Esmaiel Derafshian; Somaieh Akhoondi. "Efficient classical synthesis of aminoazines under microwave irradiation". فصلنامه علمی زیست فناوری گیاهان زراعی, 2, Issue 2, pp. 82-163, Serial No. 3, 1393, 157-163.
Vahdat, Seyed Mohammad, Mohammadzadeh, Abbas, Derafshian, Esmaiel, Akhoondi, Somaieh. (1393). 'Efficient classical synthesis of aminoazines under microwave irradiation', فصلنامه علمی زیست فناوری گیاهان زراعی, 2(Issue 2, pp. 82-163, Serial No. 3), pp. 157-163.
Vahdat, Seyed Mohammad, Mohammadzadeh, Abbas, Derafshian, Esmaiel, Akhoondi, Somaieh. Efficient classical synthesis of aminoazines under microwave irradiation. فصلنامه علمی زیست فناوری گیاهان زراعی, 1393; 2(Issue 2, pp. 82-163, Serial No. 3): 157-163.

Efficient classical synthesis of aminoazines under microwave irradiation

Iranian chemical communication
مقاله 8، دوره 2، Issue 2, pp. 82-163, Serial No. 3، تیر 2014، صفحه 157-163    اصل مقاله (223.36 K)
نوع مقاله: Original Research Article
نویسندگان
Seyed Mohammad Vahdat1؛ Abbas Mohammadzadeh* 2؛ Esmaiel Derafshian1؛ Somaieh Akhoondi1
1Department of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, P.O. Box 678, Amol, Iran
2Chemistry Research Laboratory, Faculty of Science,Ayatollah Amoli Branch, Islamic Azad University, Amol, Iran
چکیده
In the present study, Aminoazines were prepared from the reaction of amidrazone hydroiodide with various aromatic aldehydes in the presence of a solid base under microwave irradiation with power level of 850 W for 2-7 min in high yields. The amidrazone hydroiodide can also be prepared by the reaction of S-methyl isothiobenzamide hydroiodide and hydrazine in methanol under nitrogen gas. All synthesized compounds were characterized on the basis of IR and 1H NMR spectral data. The significant features of this method are short reaction times, high yields of the products, solvent free reaction, easy work-up procedure, directly production of aminoazines.
کلیدواژه‌ها
Aminoazine؛ aldehyde؛ microwave irradiation
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