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The Influence of Green Surface Modification of Magnetite Nanoparticles on the Tolid Phase Extraction Tramadol Followed by High Performance Liquid Chromatography–Diode Array Aetection | ||
| Iranian Journal of Analytical Chemistry | ||
| مقاله 7، دوره 7، شماره 2 - شماره پیاپی 14، آذر 2020، صفحه 57-66 اصل مقاله (981.33 K) | ||
| نوع مقاله: Full research article | ||
| شناسه دیجیتال (DOI): 10.30473/ijac.2021.59395.1192 | ||
| نویسندگان | ||
| Mohammad Vahidifar1؛ Zarrin Eshaghi* 1؛ Ramin Rezaee2 | ||
| 1Department of Chemistry, Payame Noor University, P.O. Box 19395-4697 Tehran, Iran | ||
| 2Clinical Research Unit, Faculty of Medicine, Mashhad University of Medical Sciences, Mashhad, Iran | ||
| چکیده | ||
| In this paper, a new rapid and sensitive method based on sodium dodecyl sulfate modified Fe3O4@α–Linolenic acid nanocomposite combined with high-performance liquid chromatography-photo diode array detection (HPLC–PDA) has been proposed for the extraction and determination of tramadol (TRA) in water samples. The Fe3O4@α–Linolenic acid NPs were synthesized and then characterized by Fourier transform-infrared spectroscopy (FT−IR), scanning electron microscopy (SEM) and X-ray diffraction (XRD). The main factors influencing extraction and desorption efficiency were optimized. Under optimum conditions, the method was successfully applied to the determination of TRA in the environmental samples and good linearity in the range of 0.1–500ng.mL-1(𝑅2> 0.99) obtained. The detection limit (LOD) and relative standard deviation (RSD) were0.074ng.mL-1 and 2.89 %( n=5) respectively. Finally, the proposed method was successfully applied with the relative recoveries percentages from 94–103.97% for the extraction and determination of tramadol in aqueous samples. | ||
| کلیدواژه‌ها | ||
| Tramadol؛ Magnetic Nanoparticle؛ Solid Phase Extraction؛ HPLC-DAD | ||
| عنوان مقاله [English] | ||
| تأثیر اصلاح سبز سطح نانوذرات مگنتیت برای استخراج فاز جامد ترامادول و به دنبال آن کروماتوگرافی مایع با عملکرد بالا با تشخیص آرایه دیودی | ||
| نویسندگان [English] | ||
| محمد وحیدیفر1؛ زرین اسحاقی1؛ رامین رضایی2 | ||
| 1گروه شیمی، دانشکده علوم پایه، دانشگاه پیام نور، تهران، ایران | ||
| 2واحد تحقیقات بالینی ، دانشکده پزشکی ، دانشگاه علوم پزشکی مشهد ، مشهد ، ایران | ||
| چکیده [English] | ||
| چکیده در این مقاله، یک روش جدید سریع و حساس مبتنی بر نانوکامپوزیت α-لینولنیک اسید Fe3O4 @ روکش دار با سدیم دودسیل سولفات همراه با کروماتوگرافی مایع با عملکرد بالا -آشکارساز آرایه دیودی (HPLC-PDA) برای استخراج و تعیین ترامادول (TRA) در نمونه های آب ارایه شده است. نانوذرات α -لینولنیک اسید Fe3O4 @ توسط طیف سنجی مادون قرمز تبدیل فوریه (FT-IR) ، میکروسکوپ الکترونی روبشی (SEM) و پراش اشعه ایکس (XRD) مشخص یابی شد. عوامل اصلی موثر بر استخراج و واجذب بهینه سازی شدند. در شرایط مطلوب ، روش با موفقیت برای تعیین TRA در نمونه های محیطی اعمال شد و خطی بودن خوب در محدوده 0.1-500 نانوگرم بر میلی لیتر (𝑅2> 0.99) بدست آمد. حد تشخیص (LOD) و انحراف استاندارد نسبی (RSD) به ترتیب 0.074نانوگرم بر میلی لیتر و 2.89٪ بود. سرانجام، روش پیشنهادی برای استخراج و تعیین ترامادول در نمونه های آبی با درصد بازیابی نسبی از 94 تا 103.97٪ با موفقیت اعمال شد. | ||
| کلیدواژه‌ها [English] | ||
| ترامادول, نانو ذره مغناطیسی, استخراج فاز جامد, HPLC-DAD | ||
| مراجع | ||
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