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Dye-Based Acceptor as a Colorimetric Chemosensor for Determination of Dual Ions, Tin (II) and Citrate Ion in Aqueous/ Dimethyl Sulfoxide Media with Analytical Applications | ||
| Iranian Journal of Analytical Chemistry | ||
| مقاله 9، دوره 7، شماره 2 - شماره پیاپی 14، آذر 2020، صفحه 75-84 اصل مقاله (805.42 K) | ||
| نوع مقاله: Full research article | ||
| شناسه دیجیتال (DOI): 10.30473/ijac.2021.59511.1199 | ||
| نویسندگان | ||
| Hossein Tavallali* ؛ Gohar Deilamy-Rad؛ Mohammad Ali Karimi؛ Elaheh Sharifi؛ Zahra Tavallali؛ Arshida Najafi-Nejad | ||
| Department of Chemistry, Payame Noor University, P.O. Box 19395-4697, Tehran, Iran | ||
| چکیده | ||
| Bromopyrogallol Red (BPR) dye (Dibromopyrogallolsulfonphthalein), was evaluated as a highly selective colorimetric chemosensor for tin and citrate ion. BPR displayed rapid response, high specificity, visual determination and good selectivity toward tin and citrate ion over other competing cations and anions in DMSO/H2O (1:1 v/v) media. The sensing mechanism was discussed by UV–Vis, titration, and a comparison study. Over a wide range from 0.4 µmol L-1 to 153.8 µmol L-1 and 0.02 µmol L-1 to 1.08 µmol L-1, a good linear relationship between the absorbance and the concentration of tin and citrate ion was found respectively and the detection limit was estimated to be as low as 0.06 and 0.003 µmol L-1 (S/N = 3) for tin and citrate ion. This proposed chemosensor has also been successfully applied for the determination of citrate in real samples which demonstrates its value of practical applications in food and biological systems. | ||
| کلیدواژه‌ها | ||
| Colorimetric Chemosensor؛ Bomopyrogallol Red Dye؛ Tin(II) Ion؛ Citrate Ion | ||
| عنوان مقاله [English] | ||
| پذیرنده بر پایه رنگ به عنوان یک حسگر شیمیایی رنگ سنجی برای تعیین دو یون: قلع (II) و آنیون سیترات در محیط های آبی / دی متیل سولفوکسید با کاربردهای تجزیه ای | ||
| نویسندگان [English] | ||
| حسین توللی؛ گوهر دیلمی راد؛ محمدعلی کریمی؛ الهه شریفی؛ زهرا توللی؛ آرشیدا نجفی نژاد | ||
| گروه شیمی، دانشکده علوم پایه، دانشگاه پیام نور، تهران، ایران | ||
| چکیده [English] | ||
| رنگ بروموپیروگالول قرمز (BPR) (دی بروموپیروگالول سولفو نفتالن )، به عنوان یک حسگر شیمیایی رنگ سنجی بسیار گزینش پذیر برای کاتیون قلع(II) و آنیون سیترات مورد ارزیابی قرار گرفت. پاسخ سریع، عملکرد اختصاصی، تعیین چشمی و گزینش پذیری مناسب برای کاتیون قلع(II) و آنیون سیترات نسبت به سایر کاتیون ها و آنیون های رقیب را در محیط دی متیل سولفوکسید/آب (v/v 1:1) نشان داد. مکانیسم شناسایی این روش به وسیله تکنیک های اسپکتروفتومتری فرابنفش-مرئی، تیتراسیون و یک مطالعه مقایسه ای مورد بحث قرار گرفت. در محدوده خطی وسیعی از 4/0 تا 8/153 میکرومول بر لیترو 02/0 تا 08/1 میکرومول لیتر با یک رابطه خطی خوب بین جذب و غلظت به ترتیب برای یون های قلع(II) و سیترات بدست آمد. حد تشخیص تخمین زده می شود برای یون قلع(II) و سیترات به ترتیب 06/0 و 003/0 میکرومول بر لیتر (S/N = 3)اندازه گیری شد. این حسگر شیمیایی پیشنهادی همچنین برای تعیین سیترات در نمونه های حقیقی که ارزش کاربردهای عملی آن را در سیستم های غذایی و بیولوژیکی نشان می دهد، با موفقیت به کار گرفته شد. | ||
| کلیدواژه‌ها [English] | ||
| حسگر رنگ سنجی شیمیایی, بروموپیروگالول قرمز, یون قلع (II), یون سیترات | ||
| مراجع | ||
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