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Arabi, Afroozeh, Mohadesi, Alireza, Karimi, Mohammad Ali, Ranjbar, Mehdi. (1400). Synthesis and Evaluation of Nano Zeolite Na/Al as a New Modifier for Electrochemical Determination of Acetaminophen. فصلنامه علمی زیست فناوری گیاهان زراعی, 9(1), 88-96. doi: 10.30473/ijac.2022.64005.1238
Afroozeh Arabi; Alireza Mohadesi; Mohammad Ali Karimi; Mehdi Ranjbar. "Synthesis and Evaluation of Nano Zeolite Na/Al as a New Modifier for Electrochemical Determination of Acetaminophen". فصلنامه علمی زیست فناوری گیاهان زراعی, 9, 1, 1400, 88-96. doi: 10.30473/ijac.2022.64005.1238
Arabi, Afroozeh, Mohadesi, Alireza, Karimi, Mohammad Ali, Ranjbar, Mehdi. (1400). 'Synthesis and Evaluation of Nano Zeolite Na/Al as a New Modifier for Electrochemical Determination of Acetaminophen', فصلنامه علمی زیست فناوری گیاهان زراعی, 9(1), pp. 88-96. doi: 10.30473/ijac.2022.64005.1238
Arabi, Afroozeh, Mohadesi, Alireza, Karimi, Mohammad Ali, Ranjbar, Mehdi. Synthesis and Evaluation of Nano Zeolite Na/Al as a New Modifier for Electrochemical Determination of Acetaminophen. فصلنامه علمی زیست فناوری گیاهان زراعی, 1400; 9(1): 88-96. doi: 10.30473/ijac.2022.64005.1238

Synthesis and Evaluation of Nano Zeolite Na/Al as a New Modifier for Electrochemical Determination of Acetaminophen

Iranian Journal of Analytical Chemistry
دوره 9، شماره 1 - شماره پیاپی 17، خرداد 2022، صفحه 88-96    اصل مقاله (1.03 M)
نوع مقاله: Full research article
شناسه دیجیتال (DOI): 10.30473/ijac.2022.64005.1238
نویسندگان
Afroozeh Arabi1؛ Alireza Mohadesi* 1؛ Mohammad Ali Karimi1؛ Mehdi Ranjbar2
1Department of Chemistry, Payame Noor University, Tehran 19395-4697, Iran
2Pharmaceutics Research Center, Institute of Neuropharmacology, Kerman University of Medical Sciences, Kerman, Iran
چکیده
In this study, a new Zeolite Al/Na (ZAN) was synthesized and characterized and then a new modified Carbon Paste Electrode with ZAN was made to determine Acetaminophen. Electrochemical studies using Linear Sweep Voltammetry and differential pulse voltammetry were used to determine electrochemical  Acetaminophen . In the presence of Acetaminophen , modified electrode with ZAN shows a specific anodic peak at ~ 0.59 volts which is the result of using electrocatalytic oxidation of  Acetaminophen . The determination limit of this method to measure  Acetaminophen was 5.8 µM, the relative standard deviation for 7 repeated measurements was 1.1 % and linear range of the calibration to measure  Acetaminophen was 10 up to 115 µM . for the characterization of ZAN nanostructures we used SEM (Scanning Electron Microscopy), DLS (Dynamic Light Scattering) and FT-IR (Fourier-Transform Infrared spectroscopy).
کلیدواژه‌ها
Zeolite Al/Na؛ Carbon Paste Electrode؛ Acetaminophen؛ Electroanalysis
عنوان مقاله [English]
سنتز و ارزیابی نانو زئولیت Na/Al به عنوان یک اصلاح‌کننده جدید برای اندازه‌گیری الکتروشیمیایی استامینوفن
نویسندگان [English]
افروزه عربی1؛ علیرضا محدثی زرندی1؛ محمدعلی کریمی1؛ مهدی رنجبر2
1گروه شیمی، دانشگاه پیام نور، صندوق پستی 3697-19395 تهران، ایران
2مرکز تحقیقات دارویی، انستیتوی نوروفورموکولوژی، دانشگاه علوم پزشکی کرمان، کرمان، ایران
چکیده [English]
در این تحیقق، نانو زئولیت‌های Na/Al (ZAN) سنتز و شناسایی شدند، سپس یک الکترود کربن اصلاح ­شده (CPE) شده با   ZAN  برای اندازه گیری استامینوفن ساخته شد. مطالعات الکتروشیمیایی با ولتامتری رفت و برگشت خطی ولتامتری پالس تفاضلی انجام شد. این الکترود اصلاح شده در حضور استامینوفن به دلیل خواص الکتروکاتالیستی، پیک اکسیداسیون خاصی را در ولتاژ 59/0ولت نشان می دهد. حد تشخیص این روش 8/5 میکرومولار، انحراف استاندارد نسبی برای 7 اندازه گیری تکراری 1/1درصد و محدوده خطی کالیبراسیون برای تعیین استامینوفن 10 تا 115 میکرومولار است.
کلیدواژه‌ها [English]
الکترود اصلاح شده, زئولیت, اندازه گیری الکتروکاتالیزوری, استامینوفن
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